Synthesis, 2DNMR and Crystal Structure Analysis of Piperidin – 4 – one Derivatives
Ramani Devi R1, Kathirvel R2, Seeni Mubarak M3, Mohamed Rabeek S4, Fazal Mohamed M.I5
1R.Ramani Devi, PG and Research, Department of Chemistry, Jamal Mohamed College Autonomous, Bharathidasan University, Tiruchirappalli (Tamil Nadu), India.
2R.Kathirvel, PG Research Scholar, Department of Chemistry, Jamal Mohamed College Autonomous, Bharathidasan University, Tiruchirappalli (Tamil Nadu), India.
3Dr. M. Seeni Mubarak, Associate Professor, PG and Research, Department of Chemistry, Jamal Mohamed College Autonomous, Tiruchirappalli (Tamil Nadu), India.
4Mohamed Rabeek S, PG Research Scholar, Department of Chemistry, Jamal Mohamed College Autonomous, Bharathidasan University, Tiruchirappalli (Tamil Nadu), India.
5Fazal Mohamed M, PG Research Scholar, Department of Chemistry, Jamal Mohamed College Autonomous, Bharathidasan University, Tiruchirappalli (Tamil Nadu), India.
Manuscript received on 11 March 2014 | Revised Manuscript received on 20 March 2014 | Manuscript Published on 30 March 2014 | PP: 1-4 | Volume-3 Issue-10, March 2014 | Retrieval Number: J15060331014/14©BEIESP
Open Access | Editorial and Publishing Policies | Cite | Mendeley | Indexing and Abstracting
© The Authors. Blue Eyes Intelligence Engineering and Sciences Publication (BEIESP). This is an open access article under the CC-BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/)
Abstract: The compounds 3-chloro-3-methyl-2,6 diphenyl piperidine-4-one(1) and 3-chloro-2,6-bis-(4-methoxy-phenyl)-3- methyl-piperidin-4-one(2) have been newly synthesized and characterized by elemental analysis, IR, 1H NMR, 13C NMR and 2D NMR. X-ray crystal structure analysis has been carried out to determine the composition and molecular structures of the two compounds. The crystal packing exhibits bond lengths and bond angles.
Keywords: 3-Chloro-3-Methyl-2,6-Diphenylpiperidin-4-One, 3- Chloro-2,6-Bis-(4-Methoxy-Phenyl)-3-Methyl-Piperidin-4-One: IR, 1H NMR,13C NMR, 2D NMR and XRD Studies.
Scope of the Article: Bio-Science and Bio-Technology