Synthesis and Characterization of [Sa(p-anisal-DA)4(H2O)2]by insitu Method
Pandian Paulraj1, Madasamy Kumar2, Arumugam Sathamraja3, Ayyar Manikandan4
1Pandian Paulraj, Assistant Professor, Department of Science & Humanities, Bharath Institute of Higher Education and Research, (Tamil Nadu), India.
2Madasamy Kumar, Department of Science & Humanities, Bharath Institute of Higher Education and Research, (Tamil Nadu), India.
3Arumugam Sathamraja, Department of Science & Humanities, Bharath Institute of Higher Education and Research, (Tamil Nadu), India.
4Ayyar Manikandan, Department of Science & Humanities, Bharath Institute of Higher Education and Research, (Tamil Nadu), India.
Manuscript received on 07 November 2019 | Revised Manuscript received on 15 December 2019 | Manuscript Published on 31 December 2019 | PP: 264-267 | Volume-9 Issue-2S4 December 2019 | Retrieval Number: B11361292S419/2019©BEIESP | DOI: 10.35940/ijitee.B1136.1292S419
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© The Authors. Blue Eyes Intelligence Engineering and Sciences Publication (BEIESP). This is an open-access article under the CC-BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/)
Abstract: The insitu synthesis of Schiff base metal complex using N-phenyl-1,4-phenylenediamine (DA), p-anisaldehyde (p-anisal) as starting materials with samarium nitrate hexahydrate (Sa(NO3)2.6H2O) as a metal precursor in the molar ratio (1:1:1 M) at room temperature. The prepared metal complex is washed with several times with ethanol and boiled water for the removal of un-reacted starting materials completely. The following techniques are used to confirm the prepared Schiff base metal complex by UV-visible spectroscopy, Fourier Transforms Infrared spectroscopy, X-ray diffraction pattern and Cyclic Voltammetry.
Keywords: Schiff base, Metal Complexes, Insitu Method, Cyclic Voltammetry.
Scope of the Article: Encryption Methods and Tools