One Pot Synthesis and Characterization of Palladium [Pd(Anil-Tolu)4 (H2O)2 ]by insitu Method
Pandian Paulraj1, Madasamy Kumar2, Arumugam Sathamraja3, Govindaswamy Padmapriya4, Ayyar Manikandan5
1Pandian Paulraj, Assistant Professor, Department of Science & Humanities, Bharath Institution of Higher Education and Research, (Tamil Nadu), India.
2Madasamy Kumar, Department of Science & Humanities, Bharath Institution of Higher Education and Research, (Tamil Nadu), India.
3Arumugam Sathamraja, Department of Science & Humanities, Bharath Institution of Higher Education and Research, (Tamil Nadu), India.
4Govindaswamy Padmapriya, Department of Science & Humanities, Bharath Institution of Higher Education and Research, (Tamil Nadu), India.
5Ayyar Manikandan, Department of Science & Humanities, Bharath Institution of Higher Education and Research, (Tamil Nadu), India.
Manuscript received on 07 November 2019 | Revised Manuscript received on 15 December 2019 | Manuscript Published on 31 December 2019 | PP: 273-276 | Volume-9 Issue-2S4 December 2019 | Retrieval Number: B11391292S419/2019©BEIESP | DOI: 10.35940/ijitee.B1139.1292S419
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© The Authors. Blue Eyes Intelligence Engineering and Sciences Publication (BEIESP). This is an open-access article under the CC-BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/)
Abstract: The insitu synthesis of Schiff base metal complex using p-toluedine (p-tolu), p-anisaldehyde (p-anisal) as starting materials with Palladium nitrate hexahydrate (Pd(NO3)2.6H2O) as a metal precursor in the molar ratio (1:1:1 M) at room temperature. The prepared metal complex is washed with several times with ethanol and boiled water for the removal of un-reacted materials completely. To confirm the prepared material by the following characterization like UV-visible spectroscopy, Fourier Transforms Infrared spectroscopy, X-ray diffraction pattern and Cyclic Voltammetry.
Keywords: Schiff base, Metal Complexes, Insitu Method, Cyclic Voltammetry.
Scope of the Article: Probabilistic Models and Methods